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Beilstein J. Org. Chem. 2011, 7, 9–12, doi:10.3762/bjoc.7.2
Graphical Abstract
Figure 1: tert-Butylsulfinamide.
Scheme 1: Synthesis of acid amide.
Figure 2: N-(tert-butylthio)-tert-butylsulfonamide.
Scheme 2: Chemical synthesis of 3.
Figure 3: ORTEP diagram of 3.
Scheme 3: Synthesis of tert-butylsulfanyl chloride.
Scheme 4: Synthesis of tert-butylsulfonamide.
Scheme 5: Proposed mechanism for rearrangement.